LOX

UniProt ID: P28300
Organism: Homo sapiens
Review Status: COMPLETE
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Gene Description

LOX is a secreted, copper- and lysine-tyrosylquinone-dependent protein-lysine 6-oxidase synthesized as a preproprotein. Extracellular proteolysis produces a mature C-terminal enzyme that oxidatively deaminates selected peptidyl lysine and hydroxylysine residues in collagen and elastin, generating aldehydes that initiate covalent cross-links and stabilize collagen fibrils and elastic fibers. Collagen targeting is regulated by precursor processing and tyrosine sulfation, while the propeptide participates in recruitment to tropoelastin before being released as the noncatalytic LOX propeptide (LOX-PP). Loss-of-function variants impair LOX activity and cause familial thoracic aortic aneurysm and dissection, consistent with an essential role in aortic-wall extracellular-matrix integrity.

Existing Annotations Review

GO Term Evidence Action Reason
GO:0004720 protein-lysine 6-oxidase activity
IBA
GO_REF:0000033
ACCEPT
Summary: LOX is a copper-dependent protein-lysine 6-oxidase; this is the core catalytic activity of the mature extracellular enzyme.
Reason: The specific reaction matches the experimentally supported oxidative deamination of lysine and hydroxylysine residues in collagen and elastin (PMID:26838787; PMID:31152061).
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
FB:FBgn0034660
FB:FBgn0039848
MGI:MGI:106096
MGI:MGI:1337004
MGI:MGI:1914823
MGI:MGI:96817
PANTHER:PTN002550804
RGD:3015
UniProtKB:P28300
UniProtKB:P58215
UniProtKB:Q05063
UniProtKB:Q95L39
UniProtKB:Q96JB6
UniProtKB:Q9Y4K0
Supporting Evidence:
file:human/LOX/LOX-uniprot.txt
Responsible for the post-translational oxidative deamination
GO:0005576 extracellular region
IBA
GO_REF:0000033
ACCEPT
Summary: LOX is secreted and its catalytic forms act in the extracellular region.
Reason: Secretion and extracellular activation are intrinsic to LOX biology; the precursor is secreted before BMP1 or ADAMTS processing (PMID:31152061).
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
MGI:MGI:106096
MGI:MGI:1337004
MGI:MGI:1914823
MGI:MGI:96817
PANTHER:PTN002550804
RGD:1308435
RGD:1308752
RGD:3015
UniProtKB:P28300
UniProtKB:P33072
UniProtKB:P58215
UniProtKB:Q08397
UniProtKB:Q9Y4K0
Supporting Evidence:
file:human/LOX/LOX-uniprot.txt
Secreted, extracellular space.
GO:0031012 extracellular matrix
IBA
GO_REF:0000033
ACCEPT
Summary: LOX acts in the extracellular matrix on collagen and elastin precursors.
Reason: Matrix localization is integral to its core cross-link initiation function and is supported by collagen-binding and elastic-fiber assembly evidence.
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
MGI:MGI:106096
MGI:MGI:96817
PANTHER:PTN008698711
RGD:1308435
RGD:1308752
RGD:3015
Supporting Evidence:
PMID:31152061
post-translationally modified by tyrosine O-sulfation and contribute to binding to collagen
GO:0035791 platelet-derived growth factor receptor-beta signaling pathway
IBA
GO_REF:0000033
KEEP AS NON CORE
Summary: LOX activity modulates PDGFR-beta-dependent signaling and chemotactic sensitivity in rat aortic smooth muscle cells, with a concordant phenotype in LOX-null mouse fibroblasts.
Reason: Direct primary evidence supports this pathway connection in rat and mouse cells (PMID:18586678), but it remains a context-dependent signaling consequence of extracellular LOX activity rather than the defining matrix-cross-linking function, and direct human-cell validation is not shown.
Propagation Review
Root cause: NO FAILURE NON CORE
Failure modes: CONTEXT OR TISSUE MISMATCH
Sources checked:
MGI:MGI:96817
PANTHER:PTN002910759
RGD:3015
Supporting Evidence:
PMID:18586678
Phosphorylated members of the PDGFR-beta-dependent signal transduction pathway, including PDGFR-beta, SHP2, AKT1, and ERK1/ERK2 (p44/42 MAPK), turned over faster in BAPN-treated than in control SMCs.
GO:0030199 collagen fibril organization
IBA
GO_REF:0000033
ACCEPT
Summary: LOX initiates collagen cross-linking required for stable collagen fibrils.
Reason: Oxidation of collagen lysines and LOX collagen binding directly support a core role in collagen fibril organization (PMID:31152061).
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
MGI:MGI:96817
PANTHER:PTN008698711
RGD:3015
UniProtKB:Q9Y4K0
Supporting Evidence:
PMID:31152061
the initial step in the formation of covalent collagen cross-links, an essential process for fibril stabilization
GO:0004720 protein-lysine 6-oxidase activity
IEA
GO_REF:0000120
ACCEPT
Summary: The automated Rhea/EC and ortholog mapping correctly assigns the core protein-lysine 6-oxidase activity.
Reason: Human LOX has direct experimental support for EC 1.4.3.13 activity (PMID:26838787; PMID:31152061).
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
UniProtKB:P16636
ensembl:ENSRNOP00000019844
UniProtKB:P28301
ensembl:ENSMUSP00000025409
RHEA:24544
EC:1.4.3.13
GO:0005507 copper ion binding
IEA
GO_REF:0000120
ACCEPT
Summary: Copper is a required cofactor of the mature LOX catalytic domain.
Reason: The family domains and conserved copper-coordinating residues support this core cofactor-binding function; human biochemical descriptions identify LOX as copper dependent (PMID:1352776).
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
UniProtKB:P16636
ensembl:ENSRNOP00000019844
InterPro:IPR001695
InterPro:IPR019828
Supporting Evidence:
PMID:1352776
Lysyl oxidase (EC 1.4.3.13) is a copper-dependent enzyme
GO:0005576 extracellular region
IEA
GO_REF:0000120
ACCEPT
Summary: Automated ortholog and subcellular-location mappings correctly place LOX extracellularly.
Reason: The precursor is secreted and processed in the extracellular space, where the mature enzyme acts.
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
UniProtKB:P28301
ensembl:ENSMUSP00000025409
UniProtKB-SubCell:SL-0112
UniProtKB-SubCell:SL-0243
Supporting Evidence:
file:human/LOX/LOX-uniprot.txt
Secreted, extracellular space.
GO:0016641 oxidoreductase activity, acting on the CH-NH2 group of donors, oxygen as acceptor
IEA
GO_REF:0000002
MODIFY
Summary: This InterPro-derived oxidoreductase term is true but less informative than LOX's specific protein-lysine 6-oxidase activity.
Reason: Replace the broad donor-class activity with the experimentally established specific reaction term.
Propagation Review
Root cause: TERM SCOPING PROBLEM
Failure modes: GRANULARITY MISMATCH
Sources checked:
InterPro:IPR001695
InterPro:IPR019828
GO:0071953 elastic fiber
IEA
GO_REF:0000117
ACCEPT
Summary: LOX is recruited to elastic fibers during elastogenesis.
Reason: The localization is consistent with direct evidence that the LOX propeptide promotes assembly of LOX onto tropoelastin and with LOX-dependent elastin cross-linking (PMID:19855011).
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
ARBA:ARBA00084594
Supporting Evidence:
PMID:19855011
FBLN4 is essential for tethering LOX to tropoelastin to facilitate cross-linking.
GO:0005515 protein binding
IPI
PMID:19570982
Differential regulation of elastic fiber formation by fibuli...
MODIFY
Summary: Recombinant full-length LOX binds several elastic-fiber extracellular matrix proteins; generic protein binding obscures that context.
Reason: The study tested full-length precursor LOX and supports binding to EFEMP2/fibulin-4, elastin, fibrillin-1, and fibulin-5 in an elastic-fiber assembly system. Replace generic protein binding with extracellular matrix protein binding; this is not evidence that the isolated mature catalytic chain binds every partner.
Propagation Review
Root cause: TERM SCOPING PROBLEM
Failure modes: GRANULARITY MISMATCH
Sources checked:
UniProtKB:O95967
UniProtKB:P15502
UniProtKB:P35555
UniProtKB:Q9UBX5
Supporting Evidence:
PMID:19570982
We have determined how they interact with tropoelastin, lysyl oxidase, and fibrillin-1
GO:0005515 protein binding
IPI
PMID:19855011
Fibulin-4 conducts proper elastogenesis via interaction with...
MODIFY
Summary: EFEMP2/fibulin-4 binds specifically to the LOX propeptide and recruits proLOX to tropoelastin.
Reason: Replace uninformative protein binding with extracellular matrix protein binding, explicitly scoped to the propeptide region of the secreted precursor rather than the mature catalytic chain.
Propagation Review
Root cause: TERM SCOPING PROBLEM
Failure modes: GRANULARITY MISMATCH
Sources checked:
UniProtKB:O95967
Supporting Evidence:
PMID:19855011
We also found a specific interaction between FBLN4 and the propeptide of LOX
GO:0005515 protein binding
IPI
PMID:21690299
The lysyl oxidase propeptide interacts with the receptor-typ...
MODIFY
Summary: The released LOX propeptide binds the intracellular phosphatase domains of PTPRK; this is a propeptide function, not an activity of mature extracellular LOX.
Reason: The experiment supports the more informative protein phosphatase binding term and specifically concerns LOX-PP residues 22-168.
Propagation Review
Root cause: TERM SCOPING PROBLEM
Failure modes: GRANULARITY MISMATCH
Sources checked:
UniProtKB:Q15262
Proposed replacements: protein phosphatase binding
Supporting Evidence:
PMID:21690299
a yeast two-hybrid assay of LOX-PP-interacting proteins identified a clone encoding the intracellular phosphatase domains of receptor-type protein tyrosine phosphatase kappa (RPTP-ΞΊ), and the interaction of the two proteins in mammalian cells was confirmed.
GO:0005515 protein binding
IPI
PMID:25118846
Nuclear translocation of lysyl oxidase is promoted by intera...
UNDECIDED
Summary: The abstract reports binding between the LOX catalytic domain and transcriptional corepressor p66beta, but the GOA WITH entity is FBLN5 and the full text is unavailable.
Reason: Curator deference is required for this experimental annotation because the cached article is abstract-only, while the explicit interactor in the abstract does not match the supporting entity recorded in GOA.
Propagation Review
Root cause: UNRESOLVED
Failure modes: SOURCE MISCITATION
Sources checked:
UniProtKB:Q9UBX5
Supporting Evidence:
PMID:25118846
the LOX catalytic domain interacts with the transcription repressor p66Ξ²
GO:0005581 collagen trimer
IEA
GO_REF:0000107
REMOVE
Summary: LOX modifies collagen trimers but is not a structural subunit of the collagen triple-helical complex.
Reason: The part_of qualifier conflates an enzyme acting on collagen with membership in the collagen trimer; direct evidence instead supports collagen binding and peptidyl-lysine oxidation.
Propagation Review
Root cause: PROPAGATION BAD
Failure modes: ROLE CONFLATION
Sources checked:
UniProtKB:P28301
ensembl:ENSMUSP00000025409
GO:0009410 response to xenobiotic stimulus
IEA
GO_REF:0000107
MARK AS OVER ANNOTATED
Summary: This rat-ortholog transfer captures a toxicological expression-response context rather than LOX's biochemical role.
Reason: A xenobiotic-responsive change in a donor organism is too contextual to define human LOX function and has no direct support in the human record.
Propagation Review
Root cause: PROPAGATION BAD
Failure modes: CONTEXT OR TISSUE MISMATCH
Sources checked:
UniProtKB:P16636
ensembl:ENSRNOP00000019844
GO:0009725 response to hormone
IEA
GO_REF:0000107
MARK AS OVER ANNOTATED
Summary: This broad hormone-response term was transferred from rat and is peripheral to human LOX function.
Reason: Donor expression or physiological response evidence does not establish that human LOX is core response machinery.
Propagation Review
Root cause: PROPAGATION BAD
Failure modes: CONTEXT OR TISSUE MISMATCH
Sources checked:
UniProtKB:P16636
ensembl:ENSRNOP00000019844
GO:0030199 collagen fibril organization
IEA
GO_REF:0000107
ACCEPT
Summary: Orthology transfer correctly captures LOX's core role in collagen fibril stabilization.
Reason: Direct human evidence shows collagen binding and initiation of covalent collagen cross-links, independently supporting the transferred process term (PMID:31152061).
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
UniProtKB:P16636
ensembl:ENSRNOP00000019844
Supporting Evidence:
PMID:31152061
the initial step in the formation of covalent collagen cross-links, an essential process for fibril stabilization
GO:0031012 extracellular matrix
IEA
GO_REF:0000120
ACCEPT
Summary: Automated ortholog mapping correctly places secreted LOX in the extracellular matrix.
Reason: Both precursor targeting and mature enzyme substrate chemistry are extracellular, and collagen-binding evidence directly supports matrix association.
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
UniProtKB:P16636
ensembl:ENSRNOP00000019844
UniProtKB:P28301
ensembl:ENSMUSP00000025409
GO:0048251 elastic fiber assembly
IEA
GO_REF:0000107
ACCEPT
Summary: LOX initiates elastin cross-linking and is recruited to tropoelastin during elastic fiber assembly.
Reason: This is a core extracellular role supported by direct fibulin-4/proLOX/tropoelastin assembly evidence and the established LOX reaction.
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
UniProtKB:P16636
ensembl:ENSRNOP00000019844
Supporting Evidence:
PMID:19855011
FBLN4 is essential for tethering LOX to tropoelastin to facilitate cross-linking.
GO:0048514 blood vessel morphogenesis
IEA
GO_REF:0000107
KEEP AS NON CORE
Summary: LOX-dependent collagen and elastin cross-linking contributes to vascular structure, but blood vessel morphogenesis is an organismal consequence rather than the enzyme's core molecular function.
Reason: Ortholog phenotypes and human aortic disease support vascular relevance while remaining downstream of the core matrix-cross-linking activity (PMID:26838787).
Propagation Review
Root cause: NO FAILURE NON CORE
Failure modes: CONTEXT OR TISSUE MISMATCH
Sources checked:
UniProtKB:P28301
ensembl:ENSMUSP00000025409
Supporting Evidence:
PMID:26838787
rare genetic variants in LOX predispose to thoracic aortic disease
GO:0048545 response to steroid hormone
IEA
GO_REF:0000107
MARK AS OVER ANNOTATED
Summary: This rat-derived steroid-hormone response is contextual and does not describe the core function of human LOX.
Reason: A transferred expression-response association is too indirect to establish LOX as response machinery in humans.
Propagation Review
Root cause: PROPAGATION BAD
Failure modes: CONTEXT OR TISSUE MISMATCH
Sources checked:
UniProtKB:P16636
ensembl:ENSRNOP00000019844
GO:0071953 elastic fiber
TAS
PMID:16893474
Elastic fibres in health and disease.
ACCEPT
Summary: LOX is associated with elastic fibers, where it initiates cross-link formation in tropoelastin.
Reason: Although the cited review cache is abstract-only, the localization is independently supported by direct LOX-fibulin-tropoelastin studies and Reactome elastin cross-linking.
Supporting Evidence:
Reactome:R-HSA-2129375
Soluble monomers of tropoelastin are cross-linked by the oxidative deamination of lysine residues, catalyzed by lysyl oxidase (LOX).
GO:0004720 protein-lysine 6-oxidase activity
EXP
PMID:26838787
LOX Mutations Predispose to Thoracic Aortic Aneurysms and Di...
ACCEPT
Summary: Disease-associated LOX variants reduce lysyl oxidase activity relative to wild type, directly supporting the core catalytic term.
Reason: The full-text human study experimentally compared enzyme activity of wild-type and mutant LOX proteins.
Supporting Evidence:
PMID:26838787
resulted in significantly lower lysyl oxidase activity when compared with the wild-type protein
GO:0060090 molecular adaptor activity
IPI
PMID:30082873
Insights into the structure and dynamics of lysyl oxidase pr...
REMOVE
Summary: The released LOX propeptide binds many molecules, but the study does not demonstrate that it bridges two or more partners as a molecular adaptor.
Reason: Pairwise binding and an interaction network do not satisfy the GO definition of adaptor activity; the evidence concerns LOX-PP, not mature catalytic LOX.
Propagation Review
Root cause: SOURCE BAD
Failure modes: ROLE CONFLATION
Sources checked:
ChEBI:16336
ChEBI:18376
ChEBI:37397
ChEBI:28304
ChEBI:28815
Supporting Evidence:
PMID:30082873
we have identified 17 new binding partners of the propeptide by label-free assays
GO:0005515 protein binding
IPI
PMID:30082873
Insights into the structure and dynamics of lysyl oxidase pr...
MODIFY
Summary: Human LOX-PP binds numerous extracellular, cell-surface, and enzyme partners, but generic protein binding is uninformative and applies to the released propeptide.
Reason: The assayed protein partners are dominated by extracellular-matrix proteins and matrix-associated enzymes, so extracellular matrix protein binding is more informative than generic protein binding. This replacement applies specifically to released LOX-PP residues 22-168, not the mature catalytic chain, and does not imply one stable complex containing all partners.
Propagation Review
Root cause: TERM SCOPING PROBLEM
Failure modes: GRANULARITY MISMATCH
Sources checked:
UniProtKB:P00747
UniProtKB:P01133
UniProtKB:P02452
UniProtKB:P02751
UniProtKB:P08123
UniProtKB:P08253
UniProtKB:P12109
UniProtKB:P13605
UniProtKB:P15502
UniProtKB:P21980
UniProtKB:Q07507
UniProtKB:Q14766
UniProtKB:Q9H6X2-2
UniProtKB:Q9Y4K0
Supporting Evidence:
PMID:30082873
We have identified 17 new partners of LOX-PP including four GAGs (chondroitin sulfate, dermatan sulfate, heparan sulfate, hyaluronan), collagen I, cross-linking and proteolytic enzymes (lysyl oxidase-like 2, transglutaminase-2, and MMP-2), one proteoglycan (fibromodulin), one matricryptin (anastellin),
GO:0036094 small molecule binding
IPI
PMID:30082873
Insights into the structure and dynamics of lysyl oxidase pr...
MODIFY
Summary: LOX-PP binds glycosaminoglycan polymers, not small molecules as defined by GO.
Reason: Hyaluronan, chondroitin sulfate, dermatan sulfate, heparan sulfate, and heparin are glycans; glycosaminoglycan binding is the correctly scoped function of the released propeptide.
Propagation Review
Root cause: TERM SCOPING PROBLEM
Failure modes: ROLE CONFLATION
Sources checked:
ChEBI:16336
ChEBI:18376
ChEBI:28304
ChEBI:28815
ChEBI:37397
Proposed replacements: glycosaminoglycan binding
Supporting Evidence:
PMID:30082873
They include four glycosaminoglycans (hyaluronan, chondroitin, dermatan and heparan sulfate)
GO:0005515 protein binding
IPI
PMID:27339457
Functional consequence of fibulin-4 missense mutations assoc...
MODIFY
Summary: EFEMP2/fibulin-4 binds the LOX propeptide; generic protein binding is less informative than extracellular matrix protein binding.
Reason: The abstract-only study directly identifies LOX-propeptide binding, so the interaction is retained with curator deference and explicitly scoped away from mature LOX.
Propagation Review
Root cause: TERM SCOPING PROBLEM
Failure modes: GRANULARITY MISMATCH
Sources checked:
UniProtKB:O95967
Supporting Evidence:
PMID:27339457
the binding of fibulin-4 to the LOX propeptide was strongly reduced by the mutation E57K
GO:0005515 protein binding
IPI
PMID:22919265
Yeast two-hybrid analysis of a human trabecular meshwork cDN...
REMOVE
Summary: This citation studies EFEMP2 binding to PITX2 and contains no LOX experiment despite the GOA WITH entity being EFEMP2.
Reason: Full text is available and contains no LOX or lysyl-oxidase mention; the LOX-EFEMP2 interaction is supported by other papers, but PMID:22919265 is a genuine source miscitation for this row.
Propagation Review
Root cause: SOURCE BAD
Failure modes: SOURCE MISCITATION
Sources checked:
UniProtKB:O95967
Supporting Evidence:
PMID:22919265
We discovered EFEMP2 as a novel PITX2-interacting protein.
GO:0004720 protein-lysine 6-oxidase activity
IDA
PMID:31152061
Differential cleavage of lysyl oxidase by the metalloprotein...
ACCEPT
Summary: Enzymatic assays directly support protein-lysine 6-oxidase activity of secreted LOX forms.
Reason: BMP1 and ADAMTS cleavage change collagen binding but retain enzyme activity; this catalytic activity belongs to the C-terminal mature enzyme rather than the released propeptide.
Supporting Evidence:
PMID:31152061
the enzyme catalyzing the initial step in the formation of covalent collagen cross-links
GO:0005518 collagen binding
IDA
PMID:31152061
Differential cleavage of lysyl oxidase by the metalloprotein...
ACCEPT
Summary: LOX directly binds collagen through a sulfated tyrosine-rich region retained in the BMP1-generated long mature form.
Reason: Solid-phase binding assays and differential cleavage establish collagen binding; additional ADAMTS2/14 cleavage removes the sulfated region and reduces binding.
Supporting Evidence:
PMID:31152061
some are post-translationally modified by tyrosine O-sulfation and contribute to binding to collagen
GO:0005576 extracellular region
IDA
PMID:31152061
Differential cleavage of lysyl oxidase by the metalloprotein...
ACCEPT
Summary: The LOX precursor is secreted and both analyzed processed enzyme forms are extracellular.
Reason: This directly supports extracellular-region localization while distinguishing secretion of proLOX from extracellular proteolytic maturation.
Supporting Evidence:
file:human/LOX/LOX-uniprot.txt
Secreted, extracellular space.
GO:0018057 peptidyl-lysine oxidation
IDA
PMID:31152061
Differential cleavage of lysyl oxidase by the metalloprotein...
ACCEPT
Summary: Mature LOX oxidizes peptidyl lysine and hydroxylysine to initiate covalent collagen cross-link formation.
Reason: This process term accurately captures the direct biochemical transformation catalyzed by the mature extracellular enzyme.
Supporting Evidence:
PMID:31152061
LOX precursor, the enzyme catalyzing the initial step in the formation of covalent collagen cross-links
GO:0004720 protein-lysine 6-oxidase activity
ISS
GO_REF:0000024
ACCEPT
Summary: Curator-reviewed similarity transfer from mouse LOX correctly assigns the conserved core catalytic activity.
Reason: Direct human enzyme assays independently confirm the transferred protein-lysine 6-oxidase activity.
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
UniProtKB:P28301
Supporting Evidence:
PMID:26838787
resulted in significantly lower lysyl oxidase activity when compared with the wild-type protein
GO:0005576 extracellular region
ISS
GO_REF:0000024
ACCEPT
Summary: Curator-reviewed transfer from mouse LOX correctly assigns extracellular localization.
Reason: Human LOX is directly shown to be secreted and extracellularly processed.
Propagation Review
Root cause: NO FAILURE CORE
Sources checked:
UniProtKB:P28301
Supporting Evidence:
file:human/LOX/LOX-uniprot.txt
Secreted, extracellular space.
GO:0048514 blood vessel morphogenesis
ISS
GO_REF:0000024
KEEP AS NON CORE
Summary: Mouse-ortholog evidence for blood vessel morphogenesis is consistent with LOX-dependent vascular matrix integrity but is downstream of the core enzyme function.
Reason: Human pathogenic variants establish aortic relevance, while morphogenesis is an organismal phenotype rather than direct catalysis.
Propagation Review
Root cause: NO FAILURE NON CORE
Failure modes: CONTEXT OR TISSUE MISMATCH
Sources checked:
UniProtKB:P28301
Supporting Evidence:
PMID:26838787
rare genetic variants in LOX predispose to thoracic aortic disease
GO:0005515 protein binding
IPI
PMID:26601954
Characterization of Microfibrillar-associated Protein 4 (MFA...
UNDECIDED
Summary: The cached abstract concerns MFAP4 interactions, but the full text needed to verify the curated LOX-MFAP4 interaction is unavailable.
Reason: Curator deference is required for this experimental IPI annotation because absence of LOX from an abstract does not establish absence from the full study; the interaction cannot be independently verified from the accessible evidence.
Propagation Review
Root cause: UNRESOLVED
Failure modes: SOURCE EVIDENCE WEAK
Sources checked:
UniProtKB:P55083
GO:0005576 extracellular region
TAS
Reactome:R-HSA-2022141
ACCEPT
Summary: Reactome places proLOX activation in the extracellular space.
Reason: The precursor is secreted extracellularly before cleavage to the mature enzyme.
Supporting Evidence:
Reactome:R-HSA-2022141
Lysyl oxidase (LOX) is secreted to the extracellular space in an inactive, proenzyme form (proLOX).
GO:0005576 extracellular region
TAS
Reactome:R-HSA-2002466
ACCEPT
Summary: Reactome correctly places LOX-catalyzed collagen lysine oxidation extracellularly.
Reason: Collagen substrate modification occurs in the extracellular matrix and is a core LOX role.
Supporting Evidence:
Reactome:R-HSA-2002466
Lysine residues can be converted to allysine by lysyl oxidase.
GO:0005576 extracellular region
TAS
Reactome:R-HSA-2129375
ACCEPT
Summary: Reactome correctly places LOX-catalyzed tropoelastin oxidation and cross-link initiation extracellularly.
Reason: Elastin cross-linking is a core action of extracellular mature LOX.
Supporting Evidence:
Reactome:R-HSA-2129375
Soluble monomers of tropoelastin are cross-linked by the oxidative deamination of lysine residues, catalyzed by lysyl oxidase (LOX).
GO:0005576 extracellular region
TAS
Reactome:R-HSA-2395340
ACCEPT
Summary: Reactome correctly places hydroxylysine-to-hydroxyallysine conversion by LOX in extracellular collagen.
Reason: The representative collagen reaction is consistent with mature LOX substrate chemistry.
Supporting Evidence:
Reactome:R-HSA-2395340
Hydroxylysines residues can be converted to hydroxyallysines by lysyl oxidase.
GO:0004720 protein-lysine 6-oxidase activity
TAS
PMID:1352776
Characterization of the human lysyl oxidase gene locus.
ACCEPT
Summary: The human locus paper explicitly identifies LOX as EC 1.4.3.13 and describes its aldehyde-generating collagen and elastin cross-linking activity.
Reason: Although the enzyme statement is background in an abstract-only gene-locus paper, it is correct and corroborated by later direct human experiments.
Supporting Evidence:
PMID:1352776
Lysyl oxidase (EC 1.4.3.13) is a copper-dependent enzyme acting principally on collagen and elastin catalyzing the formation of aldehyde cross-links.
GO:0005507 copper ion binding
TAS
PMID:1357535
The complete derived amino acid sequence of human lysyl oxid...
ACCEPT
Summary: Human LOX contains a conserved C-terminal copper-binding catalytic domain.
Reason: The sequence paper provides human-specific domain evidence and the copper-dependent chemistry is independently established; copper binding belongs to the mature catalytic chain, not LOX-PP.
Supporting Evidence:
PMID:1357535
contains the putative copper binding sites and is likely to be the catalytically active domain
GO:0036211 protein modification process
TAS
PMID:1685472
Molecular cloning of human lysyl oxidase and assignment of t...
MODIFY
Summary: Protein modification process is correct but far broader than the specific LOX-catalyzed oxidation of collagen and elastin lysines.
Reason: Replace the generic process with peptidyl-lysine oxidation, which captures the direct covalent modification initiated by mature extracellular LOX.
Proposed replacements: peptidyl-lysine oxidation
Supporting Evidence:
PMID:1685472
initiates the crosslinking of collagens and elastin by catalyzing oxidative deamination of the epsilon-amino group in certain lysine and hydroxylysine residues

Core Functions

After secretion and extracellular processing of proLOX, the mature C-terminal copper/LTQ enzyme oxidatively deaminates selected lysine and hydroxylysine side chains in collagen and elastin to allysine and hydroxyallysine. These aldehydes initiate covalent cross-link formation, thereby stabilizing collagen fibrils and elastic fibers. Substrate delivery is form- and processing-dependent: sulfated tyrosines retained in the long mature form promote collagen binding, whereas the propeptide can recruit proLOX to fibulin-4/tropoelastin assemblies before it is released. These targeting interactions are not treated as stable complex membership. The released LOX-PP is a distinct noncatalytic product, and reported tumor-cell or nuclear effects are not assigned to this extracellular catalytic activity. Human catalytic-domain variants with reduced enzyme activity predispose to thoracic aortic disease, supporting the physiological importance of this reaction for aortic-wall matrix integrity without making disease or blood-vessel morphogenesis a second molecular function.

Supporting Evidence:
  • PMID:1685472
    Lysyl oxidase (EC 1.4.3.13) initiates the crosslinking of collagens and elastin by catalyzing oxidative deamination of the epsilon-amino group in certain lysine and hydroxylysine residues.
  • PMID:1357535
    This is the first step in the covalent cross-linking of collagen and tropoelastin and results in the formation of insoluble collagen and elastic fibers in the extracellular matrix.
  • PMID:31152061
    the initial step in the formation of covalent collagen cross-links, an essential process for fibril stabilization
  • PMID:26838787
    Expression of the LOX variants p.Ser280Arg and p.Ser348Arg resulted in significantly lower lysyl oxidase activity when compared with the wild-type protein.

References

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Suggested Questions for Experts

Q: Which collagen and elastin lysine or hydroxylysine sites are modified specifically by LOX, rather than LOXL paralogs, in the normal and aneurysmal human aortic wall?

Q: How do BMP1 and ADAMTS2/14 cleavage, tyrosine sulfation, and fibulin-4-dependent recruitment control the distribution of LOX activity between collagen fibrils and elastic fibers in vivo?

Q: Does released endogenous LOX-PP have a reproducible physiological signaling function, and is any endogenous nuclear LOX pool catalytically active in normal human cells?

Suggested Experiments

Experiment: Engineer selective LOX knockout or acute degradation in primary human aortic smooth-muscle cells and matrix-producing vascular organoids, then quantify site-resolved allysine, hydroxyallysine, and mature cross-links by mass spectrometry. Compare wild-type, catalytic-dead, and disease-variant rescue while measuring LOXL expression and activity as paralog controls.

Hypothesis: LOX modifies a defined subset of collagen and elastin sites in human aortic matrix that is not redundantly oxidized by LOXL paralogs.

Type: genome editing and matrix cross-link proteomics

Experiment: Introduce endogenous cleavage-site and sulfotyrosine-site substitutions in human fibroblasts or vascular organoids, perturb EFEMP2, and use pulse-chase labeling, form-specific immunoprecipitation, proximity labeling, and collagen/elastin cross-link measurements to distinguish transient substrate targeting from stable complex formation.

Hypothesis: Proteolytic processing and tyrosine sulfation direct LOX toward collagen, whereas the intact propeptide and fibulin-4 favor tropoelastin targeting.

Type: endogenous protein processing and substrate-targeting analysis

Experiment: Tag the endogenous precursor on each side of the BMP1 cleavage site to track the mature enzyme and LOX-PP separately, quantify their extracellular and intracellular pools, and compare endogenous perturbation with matched overexpression in normal and tumor-derived cells. Test nuclear oxidase activity, Ξ²-catenin output, and rescue with secretion-defective, cleavage-resistant, and catalytic-dead alleles.

Hypothesis: Reported LOX-PP signaling and nuclear LOX phenotypes require nonphysiological overexpression and are absent at endogenous abundance in normal human cells.

Type: form-specific endogenous localization and functional analysis

Knowledge Gaps

What is not known β€” curated, literature-grounded statements of the open unknowns (the inverse of core functions).

Gap: The quantitative substrate partitioning of endogenous human LOX among collagen types, elastin, and the corresponding LOXL-family enzymes in the aortic wall is unresolved.

OPEN BIOLOGY RESIDUAL_SUBGAP

What is known: Human sequence and biochemical evidence establish oxidation of collagen and elastin substrates, and human loss-of-function variants establish aortic-disease relevance. They do not identify which native matrix sites are modified by LOX rather than another lysyl oxidase, or quantify the relative contribution of each substrate class in human aortic tissue.

Significance: Resolving enzyme-specific substrates is necessary to connect reduced LOX activity to the collagen and elastic-lamella defects that weaken the human aortic wall.

What would resolve it: Map LOX-dependent allysine, hydroxyallysine, and mature cross-links in primary human aortic matrix after selective LOX perturbation, with orthogonal control of LOXL paralog activity and rescue by wild-type or catalytic-dead LOX.

Provenance (the field's own admissions):

Gap: How BMP1 cleavage, downstream ADAMTS2/14 cleavage, tyrosine sulfation, and propeptide-mediated recruitment are coordinated to partition LOX between collagen and elastin substrates in native human tissues is not known.

OPEN BIOLOGY RESIDUAL_SUBGAP

What is known: Expressed-LOX experiments in murine skin fibroblasts and HEK293 cells show that ADAMTS2/14 processing and sulfated tyrosines affect collagen binding. Recombinant interaction studies support fibulin-4/tropoelastin targeting through the propeptide, but do not establish the timing, stoichiometry, or tissue-specific balance of these events in vivo.

Significance: Form-specific targeting may determine which extracellular-matrix substrate is cross-linked and could explain why defects in LOX processing or recruitment preferentially disrupt particular connective tissues.

What would resolve it: Quantify endogenous long and short mature LOX forms, sulfation states, and transient substrate associations in human matrix-producing cells and organoids while perturbing BMP1, ADAMTS2/14, and EFEMP2 independently.

Provenance (the field's own admissions):

Gap: The physiological functions of released LOX-PP, and whether endogenous mature LOX has any normal intracellular or nuclear activity, remain unresolved.

OPEN BIOLOGY RESIDUAL_SUBGAP

What is known: Recombinant LOX-PP binds numerous molecules in vitro and ectopic LOX-PP alters signaling in lung-cancer cells. Nuclear accumulation of the LOX catalytic domain was observed after co-expression with p66Ξ² in tumor cells, but these experiments do not demonstrate a native nuclear pool or physiological nuclear catalysis.

Significance: Separating precursor, mature-enzyme, and released-propeptide effects is essential to prevent extracellular catalytic activity from being conflated with proposed intracellular signaling roles.

What would resolve it: Use form-specific endogenous tags and cleavage-resistant alleles to track proLOX, mature LOX, and LOX-PP in normal human cells, then test whether any nuclear pool is catalytically active and required for a reproducible phenotype at endogenous levels.

Provenance (the field's own admissions):

πŸ“š Additional Documentation

Notes

(LOX-notes.md)

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